72 Hours Running Test Report for 2tph Film Sulphonation Plant of ZHONGQING YILAN
Jul 05, 2007Ⅰ. During the 72 hours running period, analysis results of product quality at control points are in TABLE 1:
TABLE 1, data sheet of analysis results
|
No. |
Date and time |
Active matter (%) |
Free oil (%) |
Free sulphonic acid (%) |
Color (klett) |
Conclusion |
|
1 |
2007-3-13 12:00 |
97.02 |
0.26 |
1.23 |
18 |
COMPLIES |
|
2 |
2007-3-13 16:00 |
97.61 |
0.17 |
1.2 |
17 |
COMPLIES |
|
3 |
2007-3-13 20:00 |
97.51 |
0.35 |
1.09 |
16 |
COMPLIES |
|
4 |
2007-3-14 00:00 |
97.5 |
0.26 |
1.03 |
16 |
COMPLIES |
|
5 |
2007-3-14 04:00 |
97.52 |
0.43 |
0.98 |
17 |
COMPLIES |
|
6 |
2007-3-14 08:00 |
97.27 |
0.43 |
0.98 |
17 |
COMPLIES |
|
7 |
2007-3-14 12:00 |
97.51 |
0.7 |
1.16 |
16 |
COMPLIES |
|
8 |
2007-3-14 16:00 |
97.44 |
0.26 |
1.19 |
13 |
COMPLIES |
|
9 |
2007-3-14 20:00 |
97.32 |
0.78 |
1.02 |
16 |
COMPLIES |
|
10 |
2007-3-15 00:00 |
97.15 |
0.61 |
1.04 |
13 |
COMPLIES |
|
11 |
2007-3-15 04:00 |
97.25 |
0.61 |
0.96 |
15 |
COMPLIES |
|
12 |
2007-3-15 08:00 |
97.24 |
0.87 |
0.87 |
14 |
COMPLIES |
|
13 |
2007-3-15 12:00 |
97.37 |
0.9 |
0.87 |
13 |
COMPLIES |
|
14 |
2007-3-15 16:00 |
97.05 |
0.43 |
1.22 |
24 |
COMPLIES |
|
15 |
2007-3-15 20:00 |
97.74 |
0.43 |
1.28 |
25 |
COMPLIES |
|
16 |
2007-3-16 00:00 |
96.92 |
0.87 |
0.93 |
19 |
COMPLIES |
|
17 |
2007-3-16 04:00 |
97.32 |
0.43 |
1.06 |
13 |
COMPLIES |
|
Average |
|
97.34 |
0.53 |
1.07 |
17 |
COMPLIES |
Ⅱ. The final analysis result of 72 running test is as TABLE 2:
TABLE 2, The final analysis result
|
No. |
Analysis Date and tank No. |
Active matter (%) |
Free oil (%) |
Free sulphonic acid (%) |
Color (klett) |
Conclusion |
|
1 |
2007-3-15 5# tank |
97.02 |
1.34 |
1.14 |
18 |
COMPLIES |
|
2 |
2007-3-17 1# tank |
96.88 |
1.29 |
1.1 |
18 |
COMPLIES |
|
Average |
2 tank sample |
96.95 |
1.315 |
1.12 |
18 |
COMPLIES |
Test conclusion: During 72 hours testing period, the analysis results in the producing time and analysis results of final product all achieve the design requirement for this plant.
Ⅲ. 72 hours consume quantity test-results are as Table 3:
TABLE 3, the design requirements and actual consume quantity
|
ITEM |
Requirements in contract (per 1 MT of LAS) |
Results tested by metering (per 1 MT of LAS) |
|
Consume quantity of LAB |
≤744.0㎏/t |
740.1㎏/t |
|
Consume quantity of sulfur |
≤106.5㎏/t |
101.4㎏/t |
|
Consume quantity of 30% liquid sodium hydrate |
≤27.0㎏/t |
13.34㎏/t |
|
Consume quantity of electric power |
≤150kwh/t |
99.3kwh/t |
|
Consume quantity of process water |
≤12t/h |
0.235 t/h |
|
Consume quantity of steam |
≤0.34 t/h |
Not tested as don’t have test instrument |
|
Consume quantity of instrument air |
≤30Nm3/h |
Not tested as don’t have test instrument |
Test conclusion：the actual test results of consume quantity （except steam and instrument items） in 72 hours running all achieve the requirement of plant design.
Ⅳ. Testing result of effluents in 72 hours running:
It’s tested by a professional inspect institution consigned by safety-production manage department. The result is as TABLE 4:
TABLE 4 DATA sheet of effluents of sulphonation plant.
|
ITEM |
Requirements in contract |
Test result |
Conclusion |
|
SO2 content in gaseous effluents |
GB16297-96 |
36mg/stere |
COMPLIES |
|
The tiptop let speed permitted |
≤11kg/h |
2.6kg/h |
COMPLIES |
|
PH value control bound of alkali waste water |
7～10 |
8 |
COMPLIES |
|
Design requirement for the noise out of blower house |
≤85分贝 |
Place 1#: 82.1db |
COMPLIES |
|
Place 2#: 82.7db |
COMPLIES |
Test conclusion: The testing results comply to standard.
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